4-formyl-2-methoxyphenyl benzenesulfonate

Base Information

• Chemical Name: 4-formyl-2-methoxyphenyl benzenesulfonate
• CAS No.: 384861-82-9
• Molecular Formula: C₁₄H₁₂O₅S
• Molecular Weight: 292.312
• Mol file: 384861-82-9.mol

Synonyms:4-formyl-2-methoxyphenyl benzenesulfonate

Chemical Property of 4-formyl-2-methoxyphenyl benzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-formyl-2-methoxyphenyl benzenesulfonate

There total 6 articles about 4-formyl-2-methoxyphenyl benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

vanillin (121-33-5,8014-42-4) + benzenesulfonyl chloride (98-09-9) → 4-formyl-2-methoxyphenyl benzenesulfonate (384861-82-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 18h; Inert atmosphere;

DOI:10.1002/anie.201409818

Reference yield:

4-hydroxy-3-(methoxymethoxy)benzaldehyde (65298-98-8) → 4-formyl-2-methoxyphenyl benzenesulfonate (384861-82-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide

2: hydrogenchloride; methanol

3: sodium hydroxide

With hydrogenchloride; methanol; sodium hydroxide;

Reference yield:

4-benzenesulfonyloxy-3-methoxymethoxy-benzaldehyde → 4-formyl-2-methoxyphenyl benzenesulfonate (384861-82-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride; methanol

2: sodium hydroxide

With hydrogenchloride; methanol; sodium hydroxide;

upstream raw materials:

vanillin

benzenesulfonyl chloride

dimethyl sulfate

methyl iodide

Downstream raw materials:

vanillin