(2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester

Base Information

Chemical Name:(2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester
CAS No.:1076206-82-0
Molecular Formula:C₁₈H₂₃F₃N₂O₄
Molecular Weight:388.387
Hs Code.:

Synonyms:(2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester

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Chemical Property of (2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester

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Technology Process of (2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester

There total 1 articles about (2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 796096-64-5
(S)-piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

: 226717-83-5
1-(bromomethyl)-2,3,5-trifluorobenzene

: 1076206-82-0
(2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16 - 24h;

Reference yield:

: 1076206-82-0
(2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester

: (2S)-4-[(2,3,5-trifluorophenyl)methyl]-2-piperazinecarboxylic acid methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 0 - 20 ℃; for 1 - 2h;

Reference yield:

: 1076206-82-0
(2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester

: 1076206-86-4
(2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl)ester

Guidance literature:: (2S)-4-[(2,3,5-trifluorophenyl)methyl]-1,2-piperazinedicarboxylic acid 1-(1,1-dimethylethyl) 2-methyl ester; With sodium hydroxide; ethanol; water; at 20 ℃;

With water; citric acid; pH=5 - 6;