[PdCl(triphenylphosphine)(κ²-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH₂Cl2

Base Information

• Chemical Name: [PdCl(triphenylphosphine)(κ²-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH₂Cl2
• CAS No.: 1422280-64-5
• Molecular Formula: CH₂Cl₂*C₄₈H₃₈ClN₄PPd
• Molecular Weight: 928.636
• Mol file: 1422280-64-5.mol

Synonyms:[PdCl(triphenylphosphine)(κ²-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH₂Cl2

Chemical Property of [PdCl(triphenylphosphine)(κ²-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH₂Cl2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [PdCl(triphenylphosphine)(κ²-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH₂Cl2

There total 1 articles about [PdCl(triphenylphosphine)(κ²-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH₂Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

dichloromethane (75-09-2) + 1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole) (1422446-56-7) + palladium diacetate (3375-31-3) + triphenylphosphine (603-35-0) + lithium chloride → [PdCl(triphenylphosphine)(κ2-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH2Cl2 (1422280-64-5)

Guidance literature:

1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole); palladium diacetate; In acetic acid; at 100 ℃; for 3h;

lithium chloride; In acetone; at 24.84 ℃; for 24h;

dichloromethane; triphenylphosphine; for 24h;

DOI:10.1016/j.jorganchem.2012.11.036

Reference yield: 85.0%

[PdCl(triphenylphosphine)(κ2-C,N-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *CH2Cl2 (1422280-64-5) + water (7732-18-5) + triphenylphosphine (603-35-0) → trans-[PdCl(triphenylphosphine)2(κ1-C-1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)(-1H))] *1.5CH2Cl2*0.5H2O

Guidance literature:

In dichloromethane; at 24.84 ℃; for 1h;

DOI:10.1016/j.jorganchem.2012.11.036

upstream raw materials:

dichloromethane

1,1'-dimethyl-2-phenylindole-3-azo-(2-phenylindole)

palladium diacetate

triphenylphosphine