3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid

Base Information

Chemical Name:3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid
CAS No.:105364-70-3
Molecular Formula:C₁₆H₁₆O₇
Molecular Weight:320.299
Hs Code.:

Synonyms:3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid

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Chemical Property of 3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid

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Technology Process of 3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid

There total 9 articles about 3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 105364-69-0
Carbonic acid ethyl ester 5-(3-hydroxy-propyl)-2-oxo-4-phenyl-2,5-dihydro-furan-3-yl ester

: 105364-70-3
3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In water; acetone; at 0 ℃;
DOI:10.1016/S0040-4039(00)84436-6

Reference yield:

jones reagent: jones reagent

: ethyl 5-(3-hydroxypropyl)-2-oxo-4-phenyl-2,5-dihydro-3-furancarboxylate

: 105364-70-3
3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid

Guidance literature:: In acetone;

Reference yield:

: 100-39-0
benzyl bromide

: 105364-70-3
3-(4-ethoxycarbonyloxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)propionic acid

Guidance literature:: Multi-step reaction with 9 steps

1: 97 percent / NaH / tetrahydrofuran / Ambient temperature

2: 99 percent / MCPBA / CH₂Cl₂ / Ambient temperature

3: EtONa / ethanol / Heating

4: 80 percent / aq. NaOH / Heating

5: 77 percent / Me₂NH, AcONa / acetic acid / 100 °C

6: 42 percent / OsO₄,NaIO₄ / dioxane / Ambient temperature

7: 96 percent / H₂ / Pd-black / ethanol

8: 92 percent / Et₃N / tetrahydrofuran / 0 °C

9: 96 percent / CrO₃, H₂SO₄ / acetone; H₂O / 0 °C

With chromium(VI) oxide; sodium periodate; osmium(VIII) oxide; sulfuric acid; hydrogen; sodium ethanolate; sodium acetate; sodium hydride; dimethyl amine; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium; In tetrahydrofuran; 1,4-dioxane; sodium hydroxide; ethanol; dichloromethane; water; acetic acid; acetone;
DOI:10.1016/S0040-4039(00)84436-6