N'-(benzenesulfonyl)-3,4-dimethoxy-5-phenylmethoxybenzohydrazide

Base Information

Chemical Name:N'-(benzenesulfonyl)-3,4-dimethoxy-5-phenylmethoxybenzohydrazide
CAS No.:51425-83-3
Molecular Formula:C22H22 N2 O6 S
Molecular Weight:442.4849
Hs Code.:
NSC Number:187784
DSSTox Substance ID:DTXSID80307125
Wikidata:Q82054468
Mol file:51425-83-3.mol

Synonyms:51425-83-3;NSC187784;DTXSID80307125;N'-(benzenesulfonyl)-3,4-dimethoxy-5-phenylmethoxybenzohydrazide;NSC-187784

Suppliers and Price of N'-(benzenesulfonyl)-3,4-dimethoxy-5-phenylmethoxybenzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N'-(benzenesulfonyl)-3,4-dimethoxy-5-phenylmethoxybenzohydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.297g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:9
Exact Mass:442.11985760
Heavy Atom Count:31
Complexity:655

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=CC(=C1)C(=O)NNS(=O)(=O)C2=CC=CC=C2)OCC3=CC=CC=C3)OC

Technology Process of N'-(benzenesulfonyl)-3,4-dimethoxy-5-phenylmethoxybenzohydrazide

There total 6 articles about N'-(benzenesulfonyl)-3,4-dimethoxy-5-phenylmethoxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 101289-41-2
3-benzyloxy-4,5-dihydroxybenzoic acid hydrazide

: 98-09-9
benzenesulfonyl chloride

: 51425-83-3
N’-(3-(benzyloxy)-4,5-dimethoxybenzoyl)benzenesulfonohydrazide

Guidance literature:: With pyridine; at 0 - 20 ℃;

Reference yield:

: 26409-24-5
methyl 3-benzyloxy-4,5-dimethoxybenzoate

: 51425-83-3
N’-(3-(benzyloxy)-4,5-dimethoxybenzoyl)benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 19.5 g / hydrazine dihydrate / ethanol / 12 h / Heating

2: pyridine / 1.) 0 deg C, 15 min, 2.) 20 deg C, 2 h

With pyridine; hydrazine hydrate; In ethanol;
DOI:10.1039/P19810002016

Reference yield:

: 79831-86-0
methyl 3-(benzyloxy)-4,5-dihydroxybenzoate

: 51425-83-3
N’-(3-(benzyloxy)-4,5-dimethoxybenzoyl)benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 3 h / Heating

2: 19.5 g / hydrazine dihydrate / ethanol / 12 h / Heating

3: pyridine / 1.) 0 deg C, 15 min, 2.) 20 deg C, 2 h

With pyridine; potassium carbonate; hydrazine hydrate; In ethanol; acetone;
DOI:10.1039/P19810002016