benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate

Base Information

Chemical Name:benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate
CAS No.:1570043-50-3
Molecular Formula:C₂₀H₂₄N₄O₃
Molecular Weight:368.436
Hs Code.:

Synonyms:benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate

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Chemical Property of benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate

Chemical Property:

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Technology Process of benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate

There total 6 articles about benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1570043-49-0
benzyl 4-(4-(cyanomethyl)pyridin-2-yl)piperazine-1-carboxylate

: 1570043-50-3
benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate

Guidance literature:: With hydrogenchloride; at 0 ℃; for 5h;

Reference yield:

: 100704-10-7
(2-chloropyridin-4-yl)methanol

: 1570043-50-3
benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / tetrahydrofuran / Reflux

2.1: N-ethyl-N,N-diisopropylamine / 48 h / 150 °C

3.1: sodium hydroxide / methanol / 20 °C

4.1: thionyl chloride / dichloromethane / 20 °C

4.2: 20 °C

5.1: dimethyl sulfoxide / 20 °C

6.1: hydrogenchloride / 5 h / 0 °C

With hydrogenchloride; thionyl chloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1570043-46-7
1-(4-((tetrahydro-2H-pyran-2-yloxy)methyl)pyridin-2-yl)piperazine

: 1570043-50-3
benzyl 4-(4-(2-imino-2-methoxyethyl)pyridin-2-yl)piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / methanol / 20 °C

2.1: thionyl chloride / dichloromethane / 20 °C

2.2: 20 °C

3.1: dimethyl sulfoxide / 20 °C

4.1: hydrogenchloride / 5 h / 0 °C

With hydrogenchloride; thionyl chloride; sodium hydroxide; In methanol; dichloromethane; dimethyl sulfoxide;