Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside

Base Information

Chemical Name:Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside
CAS No.:150161-12-9
Molecular Formula:C₁₈H₂₆O₆
Molecular Weight:338.401
Hs Code.:

Synonyms:Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside

Chemical Property:

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Technology Process of Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside

There total 4 articles about Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 82185-79-3
methyl 4-O-benzyl-2,3-O-isopropylidene-α-D-mannopyranoside

: 74-88-4
methyl iodide

: 150161-12-9
Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside

Guidance literature:: With barium dihydroxide; barium(II) oxide; In N,N-dimethyl-formamide; for 16h; Ambient temperature;
DOI:10.1016/0008-6215(93)84079-L

Reference yield:

: 100-39-0
benzyl bromide

: 150161-12-9
Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 64.1 percent / Ag₂O / dimethylformamide / 48 h / 45 °C

2: 82 percent / Bu₄NF / tetrahydrofuran / 6 h / Ambient temperature

3: 77 percent / BaO, Ba(OH)2*8H₂O / dimethylformamide / 16 h / Ambient temperature

With barium dihydroxide; tetrabutyl ammonium fluoride; barium(II) oxide; silver(l) oxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(93)84079-L

Reference yield:

: 131089-35-5
methyl 6-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-α-D-mannopyranoside

: 150161-12-9
Methyl 4-O-benzyl-2,3-di-O-isopropylidene-6-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 64.1 percent / Ag₂O / dimethylformamide / 48 h / 45 °C

2: 82 percent / Bu₄NF / tetrahydrofuran / 6 h / Ambient temperature

3: 77 percent / BaO, Ba(OH)2*8H₂O / dimethylformamide / 16 h / Ambient temperature

With barium dihydroxide; tetrabutyl ammonium fluoride; barium(II) oxide; silver(l) oxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(93)84079-L