(1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose

Base Information

Chemical Name:(1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose
CAS No.:1418182-82-7
Molecular Formula:C₁₉H₂₄N₂O₆
Molecular Weight:376.409
Hs Code.:

Synonyms:(1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose

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Chemical Property of (1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose

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Technology Process of (1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose

There total 10 articles about (1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1418182-83-8
C₂₀H₂₈N₂O₇

: 1418182-82-7
(1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose

Guidance literature:: With sulfuric acid; at 90 ℃; for 3h;
DOI:10.1016/j.tet.2012.11.016

Reference yield:

: 1418182-81-6
(1′S,2′R,3′R,4′R)-1′-[(N-3-methoxy-2-methylacryoyl)ureido]-2′-methoxy-1′-phenyl-3′,5′-O-tetraisopropyldisiloxy-ribose

: 1418182-82-7
(1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h

2: sulfuric acid / 3 h / 90 °C

With sulfuric acid; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/j.tet.2012.11.016

Reference yield:

: 1418182-78-1
(1′S,2′R,3′R,4′R)-1′-(2-formylethyl)-2′-methoxy-1′-phenyl-3′,5′-O-tetraisopropyldisiloxyribose

: 1418182-82-7
(1′S,2′R,3′R,4′R)-1′-[(3,4-dihydro-2,4-dioxo-5-methyl-1(2H)pyrimidinyl)]-2′-methoxy-1′-phenylribose

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine; hydroxylamine hydrochloride / ethanol / 16 h / 70 °C

2: nickel dichloride; sodium tetrahydroborate / methanol / 2 h / -78 °C

3: benzene / 5 h

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h

5: sulfuric acid / 3 h / 90 °C

With pyridine; sodium tetrahydroborate; sulfuric acid; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; nickel dichloride; In tetrahydrofuran; methanol; ethanol; benzene;
DOI:10.1016/j.tet.2012.11.016