n-butyl tosylcarbamate

Base Information

• Chemical Name: n-butyl tosylcarbamate
• CAS No.: 31224-37-0
• Molecular Formula: C₁₂H₁₇NO₄S
• Molecular Weight: 271.337
• Mol file: 31224-37-0.mol

Synonyms:n-butyl tosylcarbamate

Chemical Property of n-butyl tosylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of n-butyl tosylcarbamate

There total 5 articles about n-butyl tosylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyl tosylcarbamate (14437-03-7) + butan-1-ol (71-36-3) → n-butyl tosylcarbamate (31224-37-0)

Guidance literature:

at 160 ℃; Temperature; Microwave irradiation; Flow reactor;

DOI:10.1021/acs.oprd.5b00323

Reference yield: 82.0%

4-toluenesulfonyl azide (941-55-9) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) + butan-1-ol (71-36-3) → n-butyl tosylcarbamate (31224-37-0)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; at 75 ℃; for 20h;

DOI:10.1021/acs.joc.5b02755

Reference yield:

methyl tosylcarbamate (14437-03-7) + butan-1-ol (71-36-3) → n-butyl tosylcarbamate (31224-37-0) + toluene-4-sulfonamide (70-55-3)

Guidance literature:

at 120 ℃; for 0.333333h; Sealed tube; Microwave irradiation;

DOI:10.1016/j.tetlet.2016.02.071

upstream raw materials:

methyl tosylcarbamate

butan-1-ol

toluene-4-sulfonamide

4-toluenesulfonyl azide

Downstream raw materials:

Tosylurethane