benzyl perfluoroisopropyl sulfide

Base Information

• Chemical Name: benzyl perfluoroisopropyl sulfide
• CAS No.: 68409-03-0
• Molecular Formula: C₁₀H₇F₇S
• Molecular Weight: 292.22
• Mol file: 68409-03-0.mol

Synonyms:benzyl perfluoroisopropyl sulfide

Chemical Property of benzyl perfluoroisopropyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of benzyl perfluoroisopropyl sulfide

There total 6 articles about benzyl perfluoroisopropyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

tris(dimethylamino)sulfonium 1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethanethiolate + benzyl bromide (100-39-0) → benzyl perfluoroisopropyl sulfide (68409-03-0)

Guidance literature:

In ice-water; acetonitrile;

Reference yield: 66.0%

2,2,4,4-Tetrakis(trifluoromethyl)-1,3-dithietane (791-50-4) + benzyl chloride (100-44-7) → benzyl perfluoroisopropyl sulfide (68409-03-0)

Guidance literature:

With cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1007/BF00957165

Reference yield: 37.0%

perfluoropropylene (116-15-4,13429-24-8,25120-07-4,6792-31-0) + benzyl thiocyanate (3012-37-1) → benzyl perfluoroisopropyl sulfide (68409-03-0)

Guidance literature:

With potassium fluoride; cesium fluoride; In sulfolane; at 100 ℃; autoclave;

DOI:10.1021/jo00322a047

upstream raw materials:

heptafluoropropane-2-sulphenic acid chloride

toluene

perfluoropropylene

benzyl thiocyanate

Downstream raw materials:

heptafluoropropane-2-sulphenic acid chloride

benzyl chloride