4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

Base Information

Chemical Name:4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide
CAS No.:1303518-39-9
Molecular Formula:C₁₃H₁₇F₃N₂O₂Si
Molecular Weight:318.371
Hs Code.:

Synonyms:4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

Chemical Property:

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Technology Process of 4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

There total 4 articles about 4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1303518-38-8
4-formyl-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

: 1303518-39-9
4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; at 20 ℃;

Reference yield:

: 1303518-36-6
4-(dibromomethyl)-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

: 1303518-39-9
4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: silver nitrate / ethanol; water / 2 h / Reflux

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 °C

With hydroxylamine hydrochloride; sodium acetate; silver nitrate; In ethanol; water;

Reference yield:

: 1303518-35-5
4-dibromomethyl-3-trifluoromethyl-benzoic acid

: 1303518-39-9
4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

2: silver nitrate / ethanol; water / 2 h / Reflux

3: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 °C

With hydroxylamine hydrochloride; sodium acetate; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane; water;