4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide

Base Information

Chemical Name:4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide
CAS No.:1303518-41-3
Molecular Formula:C₁₃H₁₅F₃N₂SSi
Molecular Weight:316.422
Hs Code.:

Synonyms:4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide

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Chemical Property of 4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide

Chemical Property:

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Technology Process of 4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide

There total 6 articles about 4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1303518-40-2
4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

: 1303518-41-3
4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide

Guidance literature:: With Lawessons reagent; In toluene; at 85 ℃; for 1h;

Reference yield:

: 1303518-38-8
4-formyl-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

: 1303518-41-3
4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 °C

2: methanesulfonyl chloride / 1,2-dichloro-ethane / 5.33 h / Cooling with ice; Reflux

3: Lawessons reagent / toluene / 1 h / 85 °C

With Lawessons reagent; hydroxylamine hydrochloride; sodium acetate; methanesulfonyl chloride; In ethanol; water; 1,2-dichloro-ethane; toluene;

Reference yield:

: 1303518-39-9
4-[(E)-(hydroxyimino)methyl]-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzamide

: 1303518-41-3
4-cyano-3-(trifluoromethyl)-N-[(trimethylsilyl)methyl]benzenecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonyl chloride / 1,2-dichloro-ethane / 5.33 h / Cooling with ice; Reflux

2: Lawessons reagent / toluene / 1 h / 85 °C

With Lawessons reagent; methanesulfonyl chloride; In 1,2-dichloro-ethane; toluene;