Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester

Base Information

Chemical Name:Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester
CAS No.:205238-30-8
Molecular Formula:C₁₉H₁₉NO₅S
Molecular Weight:373.43
Hs Code.:

Synonyms:Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester

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Chemical Property of Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester

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Technology Process of Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester

There total 3 articles about Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108-05-4,9003-20-7
vinyl acetate

: 205238-29-5
2-(1-Benzenesulfonyl-1H-indol-3-yl)-propane-1,3-diol

: 205238-30-8
Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester

Guidance literature:: With lipase AK; In benzene; Ambient temperature;
DOI:10.3987/com-97-s39

Reference yield:

: 80360-14-1
3-iodo-1-phenylsulfonyl-1H-indole

: 205238-30-8
Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Pd(OAc)2, Ph₃P, n-Bu₄NCl, KOAc / dimethylformamide / 80 °C

2: 53 percent / O₃, sodium borohydride / ethanol / -78 - 0 °C

3: 82 percent / lipase AK / benzene / Ambient temperature

With palladium diacetate; sodium tetrahydroborate; lipase AK; tetrabutyl-ammonium chloride; potassium acetate; ozone; triphenylphosphine; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.3987/com-97-s39

Reference yield:

: 205238-28-4
1-Benzenesulfonyl-3-(2-tert-butyl-4,5-dihydro-[1,3]dioxepin-5-yl)-1H-indole

: 205238-30-8
Acetic acid (S)-2-(1-benzenesulfonyl-1H-indol-3-yl)-3-hydroxy-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / O₃, sodium borohydride / ethanol / -78 - 0 °C

2: 82 percent / lipase AK / benzene / Ambient temperature

With sodium tetrahydroborate; lipase AK; ozone; In ethanol; benzene;
DOI:10.3987/com-97-s39