1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone

Base Information

Chemical Name:1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone
CAS No.:1310045-86-3
Molecular Formula:C₂₂H₃₂O₃
Molecular Weight:344.494
Hs Code.:

Synonyms:1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone

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Chemical Property of 1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone

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Technology Process of 1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone

There total 6 articles about 1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1310045-82-9
(2''S)-N-{1-[(1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-en-1-yl]ethylidene}-2''-(methoxymethyl)-pyrrolidin-1''-amine

: 1310045-86-3
1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone

Guidance literature:: With oxalic acid; In diethyl ether; water; at 20 ℃; for 96h;
DOI:10.1021/jo200796b

Reference yield:

: 3410-84-2
2,6-dimethoxy-4-pentylbenzaldehyde

: 1310045-86-3
1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / water

2: tetrahydrofuran

3: hydroquinone / ethanol / 36 h / 21 °C / 6750680 Torr

4: sodium methylate / methanol / 22 h / 22 °C / Inert atmosphere

5: toluene-4-sulfonic acid / n-heptane / 47 h / 100 °C

6: oxalic acid / diethyl ether; water / 96 h / 20 °C

With sodium methylate; oxalic acid; toluene-4-sulfonic acid; hydroquinone; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; n-heptane; water; 1: Aldol condensation / 2: Wittig reaction / 3: Diels-Alder reaction;
DOI:10.1021/jo200796b

Reference yield:

: 7663-54-9
2',6'-dimethoxy-1'-((E)-3-methylbuta-1,3-dienyl)-4'-pentylbenzene

: 1310045-86-3
1-((1S,2S)-2-(2',6'-dimethoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: hydroquinone / ethanol / 36 h / 21 °C / 6750680 Torr

2: sodium methylate / methanol / 22 h / 22 °C / Inert atmosphere

3: toluene-4-sulfonic acid / n-heptane / 47 h / 100 °C

4: oxalic acid / diethyl ether; water / 96 h / 20 °C

With sodium methylate; oxalic acid; toluene-4-sulfonic acid; hydroquinone; In methanol; diethyl ether; ethanol; n-heptane; water; 1: Diels-Alder reaction;
DOI:10.1021/jo200796b