2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol

Base Information

Chemical Name:2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol
CAS No.:1310045-89-6
Molecular Formula:C₂₂H₃₄O₃
Molecular Weight:346.51
Hs Code.:

Synonyms:

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Chemical Property of 2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol

Chemical Property:

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Technology Process of 2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol

There total 8 articles about 2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₆O₃

: 1310045-89-6
2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol

Guidance literature:: With sodium thiomethoxide; In N,N-dimethyl-formamide; at 140 ℃; for 3h;
DOI:10.1021/jo200796b

Reference yield:

: 3410-84-2
2,6-dimethoxy-4-pentylbenzaldehyde

: 1310045-89-6
2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydroxide / water

2: tetrahydrofuran

3: hydroquinone / ethanol / 36 h / 21 °C / 6750680 Torr

4: sodium methylate / methanol / 22 h / 22 °C / Inert atmosphere

5: toluene-4-sulfonic acid / n-heptane / 47 h / 100 °C

6: oxalic acid / diethyl ether; water / 96 h / 20 °C

7: diethyl ether; toluene / 1.5 h / 60 °C

8: sodium thiomethoxide / N,N-dimethyl-formamide / 3 h / 140 °C

With sodium methylate; oxalic acid; toluene-4-sulfonic acid; hydroquinone; sodium hydroxide; sodium thiomethoxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; n-heptane; water; N,N-dimethyl-formamide; toluene; 1: Aldol condensation / 2: Wittig reaction / 3: Diels-Alder reaction / 7: Grignard reaction;
DOI:10.1021/jo200796b

Reference yield:

: 3411-09-4
(E)-4-(2,6-dimethoxy-4-pentylphenyl)but-3-en-2-one

: 1310045-89-6
2-((1S,2S)-2-(2'-hydroxy-6'-methoxy-4'-pentylphenyl)-4-methylcyclohex-3-enyl)propan-2-ol

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran

2: hydroquinone / ethanol / 36 h / 21 °C / 6750680 Torr

3: sodium methylate / methanol / 22 h / 22 °C / Inert atmosphere

4: toluene-4-sulfonic acid / n-heptane / 47 h / 100 °C

5: oxalic acid / diethyl ether; water / 96 h / 20 °C

6: diethyl ether; toluene / 1.5 h / 60 °C

7: sodium thiomethoxide / N,N-dimethyl-formamide / 3 h / 140 °C

With sodium methylate; oxalic acid; toluene-4-sulfonic acid; hydroquinone; sodium thiomethoxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; n-heptane; water; N,N-dimethyl-formamide; toluene; 1: Wittig reaction / 2: Diels-Alder reaction / 6: Grignard reaction;
DOI:10.1021/jo200796b