C₂₂H₂₅BrN₂O₅S

Base Information

Chemical Name:C₂₂H₂₅BrN₂O₅S
CAS No.:1434643-49-8
Molecular Formula:C₂₂H₂₅BrN₂O₅S
Molecular Weight:509.421
Hs Code.:

C<sub>22</sub>H<sub>25</sub>BrN<sub>2</sub>O<sub>5</sub>S

Synonyms:C₂₂H₂₅BrN₂O₅S

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Chemical Property of C₂₂H₂₅BrN₂O₅S

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Technology Process of C₂₂H₂₅BrN₂O₅S

There total 11 articles about C₂₂H₂₅BrN₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1434643-44-3
C₂₆H₃₃BrN₂O₅S

: 1434643-49-8
C₂₂H₂₅BrN₂O₅S

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 4815-30-9
diethyl 5-amino-3-methyl-2,4-thiophenedicarboxylate

: 1434643-49-8
C₂₂H₂₅BrN₂O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C

1.2: 10 - 100 °C

2.1: sodium hydroxide; water / methanol / 4 h / 50 °C

3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C

4.1: bromine; CH₃COONa / acetic acid / 1 h / 20 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 20 °C

With 1-methyl-pyrrolidin-2-one; di-isopropyl azodicarboxylate; CH₃COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetic acid;

Reference yield:

: 1434655-18-1
tert-butyl 2-isocyanato-2-methylpropanoate

: 1434643-49-8
C₂₂H₂₅BrN₂O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C

1.2: 10 - 100 °C

2.1: sodium hydroxide; water / methanol / 4 h / 50 °C

3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C

4.1: bromine; CH₃COONa / acetic acid / 1 h / 20 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 20 °C

With 1-methyl-pyrrolidin-2-one; di-isopropyl azodicarboxylate; CH₃COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetic acid;