C₁₅H₁₉FO

Base Information Edit

Chemical Name:C₁₅H₁₉FO
CAS No.:1198223-32-3
Molecular Formula:C₁₅H₁₉FO
Molecular Weight:234.314
Hs Code.:
Mol file:1198223-32-3.mol

Synonyms:C₁₅H₁₉FO

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Chemical Property of C₁₅H₁₉FO Edit

Chemical Property:

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Technology Process of C₁₅H₁₉FO

There total 6 articles about C₁₅H₁₉FO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1198223-31-2
C₁₄H₁₇FO₂

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1198223-32-3
C₁₅H₁₉FO

Guidance literature:: Methyltriphenylphosphonium bromide; With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.5h;

C₁₄H₁₇FO₂; In tetrahydrofuran; at -78 - 20 ℃; for 3h;

Reference yield:

: 51446-31-2
4-fluoro-3-hydroxybenzoic acid

: 1198223-32-3
C₁₅H₁₉FO

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / 4 h / 105 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 125 °C

3.1: water; sodium hydroxide / ethanol / 3 h / 55 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 20 °C

4.2: 13 h / 20 °C

5.1: tetrahydrofuran / 2.5 h / 0 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

6.2: 3 h / -78 - 20 °C

With sulfuric acid; water; sodium hexamethyldisilazane; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 351317-28-7
ethyl 3-hydroxy-4-fluorobenzoate

: 1198223-32-3
C₁₅H₁₉FO

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 125 °C

2.1: water; sodium hydroxide / ethanol / 3 h / 55 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 20 °C

3.2: 13 h / 20 °C

4.1: tetrahydrofuran / 2.5 h / 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

5.2: 3 h / -78 - 20 °C

With water; sodium hexamethyldisilazane; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;