bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane

Base Information

• Chemical Name: bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane
• CAS No.: 1259224-81-1
• Molecular Formula: C₁₉H₂₀N₈O₂S₂
• Molecular Weight: 456.552

Synonyms:bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane

Chemical Property of bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane

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Technology Process of bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane

There total 1 articles about bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

5-(3-carboxy-4-methoxybenzyl)-2-methoxybenzoic acid (227595-84-8) + Thiocarbohydrazide (2231-57-4) → bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane (1259224-81-1)

Guidance literature:

Heating;

Reference yield: 84.0%

bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane (1259224-81-1) + 4-Nitrophenacyl bromide (99-81-0) → bis[4-methoxy-3-(6-(4-nitrophenyl)-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazin-3-yl)phenyl]methane

Guidance literature:

In ethanol; for 6h; Reflux;

DOI:10.17344/acsi.2015.2124

Reference yield: 82.0%

bis[4-methoxy-3-[4-amino-5-sulfanyl-4H-1,2,4-triazole-3-yl]phenyl]methane (1259224-81-1) + α-bromoacetophenone (70-11-1) → bis[4-methoxy-3-(6-phenyl-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazin-3-yl)phenyl]methane

Guidance literature:

In ethanol; for 6h; Reflux;

DOI:10.17344/acsi.2015.2124

upstream raw materials:

5-(3-carboxy-4-methoxybenzyl)-2-methoxybenzoic acid

Thiocarbohydrazide

Downstream raw materials:

bis[4-methoxy-3-(6-(4-chlorobenzyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol)phenyl]methane

bis[4-methoxy-3-(6-benzyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol)phenyl]methane

bis[4-methoxy-3-(6-(4-methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol)phenyl]methane

bis[4-methoxy-3-(6-(4-methoxyphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol)phenyl]methane

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