Methyl 2-(carbamoylamino)-5-iodobenzoate

Base Information

Chemical Name:Methyl 2-(carbamoylamino)-5-iodobenzoate
CAS No.:116027-11-3
Molecular Formula:C₉H₉IN₂O₃
Molecular Weight:320.087
Hs Code.:
DSSTox Substance ID:DTXSID101248387

Synonyms:116027-11-3;DTXSID101248387;Methyl 2-[(aminocarbonyl)amino]-5-iodobenzoate

Suppliers and Price of Methyl 2-(carbamoylamino)-5-iodobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-(carbamoylamino)-5-iodobenzoate

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:319.96579
Heavy Atom Count:15
Complexity:260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC(=O)C1=C(C=CC(=C1)I)NC(=O)N

Technology Process of Methyl 2-(carbamoylamino)-5-iodobenzoate

There total 3 articles about Methyl 2-(carbamoylamino)-5-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 590-28-3
potassium cyanate

: 77317-55-6
methyl 2-amino-5-iodobenzoate

: 116027-11-3
N-<4-iodo-2-(methoxycarbonyl)phenyl>urea

Guidance literature:: In water; acetic acid; Heating;
DOI:10.1021/jm00119a014

Reference yield:

: 116027-10-2
5-iodoisatoic anhydride

: 116027-11-3
N-<4-iodo-2-(methoxycarbonyl)phenyl>urea

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 4-(dimethylamino)pyridine / methanol / 3 h / 60 °C

2: 70 percent / H₂O; acetic acid / Heating

With dmap; In methanol; water; acetic acid;
DOI:10.1021/jm00119a014

Reference yield:

: 5326-47-6
2-amino-5-iodobenzoic acid

: 116027-11-3
N-<4-iodo-2-(methoxycarbonyl)phenyl>urea

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / dioxane / 60 °C

2: 97 percent / 4-(dimethylamino)pyridine / methanol / 3 h / 60 °C

3: 70 percent / H₂O; acetic acid / Heating

With dmap; In 1,4-dioxane; methanol; water; acetic acid;
DOI:10.1021/jm00119a014