trans-Cl₂Pd(PheOMe)2

Base Information

Chemical Name:trans-Cl₂Pd(PheOMe)2
CAS No.:89973-66-0
Molecular Formula:C₂₀H₂₆Cl₂N₂O₄Pd
Molecular Weight:535.763
Hs Code.:

Synonyms:trans-Cl₂Pd(PheOMe)2

Suppliers and Price of trans-Cl₂Pd(PheOMe)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-Cl₂Pd(PheOMe)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-Cl₂Pd(PheOMe)2

There total 2 articles about trans-Cl₂Pd(PheOMe)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: sodium tetrachloropalladate(II)

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 89973-66-0
trans-Cl₂Pd(PheOMe)2

Guidance literature:: With sodium acetate; In water; under Ar or N2, Pd-complex was added to mixt. of 2 equiv. of amino-acidand 2 equiv. of NaOOCCH3, 1 h; ppt. was filtered off, dried in high vac.;
DOI:10.1515/znb-2002-0304

Reference yield: 21.0%

: potassium hexachloropalladate

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 89973-66-0
trans-Cl₂Pd(PheOMe)2

Guidance literature:: With sodium hydroxide; In water; aq. soln. of K2PdCl6 and amino-acid was stirred and to the mixt. was dropped 1 N NaOH within 20 min, stirring was continued for 18 h; soln. was filtered, residue was washed with water, then ethanol and ether and dried in vac. over P2O5; elem. anal.;

Reference yield: 88.0%

: 14104-20-2
silver tetrafluoroborate

: 89973-66-0
trans-Cl₂Pd(PheOMe)2

: trans-[methyl-(L)-phenylalaninate]2Pd(BF₄)2

Guidance literature:: In dichloromethane; byproducts: AgCl; under Ar or N2, with exlusion of light, 2 equiv. of AgBF4 was added to CH2Cl2 soln. of Pd-complex, stirring for 15 min; ppt. was centrifuged off, solvent was removed in vac., elem. anal., MeOH, MeCN and Me2CO not good solvents for this reaction;
DOI:10.1515/znb-2002-0304