4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone

Base Information

Chemical Name:4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone
CAS No.:1354708-13-6
Molecular Formula:C₃₀H₄₂O₈
Molecular Weight:530.659
Hs Code.:

Synonyms:4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone

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Chemical Property of 4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone

Chemical Property:

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Technology Process of 4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone

There total 3 articles about 4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 72023-44-0
2,3,4,5-tetramethoxybenzoic acid

: 649551-92-8
2'-hydroxy-4'-decyl-2-methoxy-acetophenone

: 1354708-13-6
4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1139/v11-087

Reference yield:

: 118-41-2
Eudesmic acid

: 1354708-13-6
4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / chloroform / Inert atmosphere

2: copper / methanol / Inert atmosphere

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With dmap; bromine; copper; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; chloroform;
DOI:10.1139/v11-087

Reference yield:

: 23346-82-9
2-bromo-3,4,5-trimethoxybenzoic acid

: 1354708-13-6
4'-decyl-2-methoxy-2'-(2'',3'',4'',5''-tetramethoxybenzoyloxy)acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: copper / methanol / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With dmap; copper; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1139/v11-087