2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine

Base Information

Chemical Name:2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine
CAS No.:1332302-39-2
Molecular Formula:C₁₆H₁₆ClF₃N₄O₂
Molecular Weight:388.777
Hs Code.:

Synonyms:2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine

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Chemical Property of 2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine

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Technology Process of 2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine

There total 4 articles about 2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 2831-66-5
2,4-dichloro-1,3,5-triazine

: 1211875-20-5
4-(4-(trifluoromethoxy)benzyloxy)piperidine trifluoroacetate salt

: 1332302-39-2
2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In isopropyl alcohol; at 80 ℃; for 2h;

Reference yield:

: 50824-05-0
4-trifluoromethoxybenzyl bromide

: 1332302-39-2
2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C / Cooling with ice

1.2: 15 h / 20 °C / Cooling with ice

2.1: dichloromethane / 2 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 2 h / 80 °C

With sodium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; mineral oil;

Reference yield:

: 287952-21-0
4-[(4-trifluoromethoxy)phenyl]methoxypiperidine-1-formic acid tert-butyl ester

: 1332302-39-2
2-chloro-4-(4-((4-(trifluoromethoxy)benzyl)oxy)piperidin-1-yl)-1,3,5-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 2 h / 80 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane; isopropyl alcohol;