Technology Process of C32H39N5O7S
There total 7 articles about C32H39N5O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2,4-Dimethoxybenzylamine; C23H26N4O6S;
In
ethanol; toluene;
for 18h;
Molecular sieve;
Reflux;
With
methanol; sodium tetrahydroborate;
at 0 ℃;
for 0.166667h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrahydrofuran / 3 h / 20 - 30 °C
2.1: iodine; ammonium cerium (IV) nitrate / acetonitrile / 20 h / 20 °C
3.1: potassium carbonate / acetonitrile / 60 °C
4.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C
5.1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
6.1: toluene; ethanol / 18 h / Molecular sieve; Reflux
6.2: 0.17 h / 0 °C
With
potassium phosphate; n-butyllithium; ammonium cerium (IV) nitrate; iodine; potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetonitrile / 60 °C
2.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C
3.1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
4.1: toluene; ethanol / 18 h / Molecular sieve; Reflux
4.2: 0.17 h / 0 °C
With
potassium phosphate; n-butyllithium; potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene; acetonitrile;