3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine

Base Information

Chemical Name:3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine
CAS No.:1634649-12-9
Molecular Formula:C₂₁H₂₄N₆O₃
Molecular Weight:408.46
Hs Code.:

Synonyms:3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine

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Chemical Property of 3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine

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Technology Process of 3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine

There total 5 articles about 3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.6%

: 17061-85-7
1-nitro-4-(prop-2-ynyloxy)benzene

: 1634649-04-9
N-sec-butyl-3-(azidomethyl)benzamidine

: 1634649-12-9
3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 60 ℃; for 48h;
DOI:10.3390/molecules19055674

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1634649-12-9
3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 3.75 h / 20 °C / Reflux

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 48 h / 60 °C

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; In water; acetone; tert-butyl alcohol;
DOI:10.3390/molecules19055674

Reference yield:

: 28188-41-2
m-(bromomethyl)benzonitrile

: 1634649-12-9
3-((4-((4-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N-sec-butylbenzamidine

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / N,N-dimethyl-formamide; water / 1.5 h / 10 - 30 °C

2: hydrogenchloride / 168 h / 20 °C / Cooling with ice

3: methanol / 30 °C

4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 48 h / 60 °C

With hydrogenchloride; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In methanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2: |Pinner Amidine Synthesis;
DOI:10.3390/molecules19055674