2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile

Base Information

Chemical Name:2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile
CAS No.:1369255-73-1
Molecular Formula:C₁₅H₉ClF₃NO₂
Molecular Weight:327.69
Hs Code.:

Synonyms:2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile

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Chemical Property of 2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile

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Technology Process of 2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile

There total 4 articles about 2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1354962-25-6
2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-formylbenzonitrile

: 1369255-73-1
2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile

Guidance literature:: With sodium tetrahydroborate; ethanol; at 20 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 6294-93-5
4-chloro-3-trifluoromethylphenol

: 1369255-73-1
2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: sodium tetrahydroborate; methanol / 0.5 h / 0 - 20 °C

With methanol; sodium tetrahydroborate; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 218301-22-5
2-fluoro-5-formylbenzonitrile

: 1369255-73-1
2-(4-chloro-3-(trifluoromethyl)phenoxy)-5-(hydroxymethyl)benzylnitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: sodium tetrahydroborate; methanol / 0.5 h / 0 - 20 °C

With methanol; sodium tetrahydroborate; potassium carbonate; In N,N-dimethyl-formamide;