(2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

Base Information

Chemical Name:(2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate
CAS No.:1433545-74-4
Molecular Formula:C₁₈H₂₃NO₅
Molecular Weight:333.384
Hs Code.:

Synonyms:(2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

Suppliers and Price of (2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

Chemical Property:

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Technology Process of (2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

There total 6 articles about (2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1433545-62-0
4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

: 1433545-74-4
(2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

Guidance literature:: With ammonium acetate; In propan-1-ol; ethanol; at 50 ℃; for 1h; Inert atmosphere; Large scale;

Reference yield:

: 1433545-53-9
ethyl 2-chloro-4-cyclobutyl-3-oxobutanoate

: 1433545-74-4
(2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 14 h / 55 °C / Inert atmosphere; Large scale

2: ammonium acetate / propan-1-ol; ethanol / 1 h / 50 °C / Inert atmosphere; Large scale

With ammonium acetate; triethylamine; In propan-1-ol; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 4415-82-1
cyclobutanemethanol

: 1433545-74-4
(2E)-3-amino-4-cyclobutyl-1-ethoxy-1-oxobut-2-en-2-yl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 4.17 h / -10 - -5 °C / Large scale

2.1: dimethyl sulfoxide / 4.67 h / 85 °C / Inert atmosphere; Large scale

3.1: zinc; chloro-trimethyl-silane / tetrahydrofuran / 4 h / 70 °C / Inert atmosphere; Large scale

3.2: 1 h / 20 °C / Large scale

4.1: sulfuryl dichloride / tert-butyl methyl ether / 1.5 h / 20 - 23 °C / Large scale

5.1: triethylamine / N,N-dimethyl-formamide / 14 h / 55 °C / Inert atmosphere; Large scale

6.1: ammonium acetate / propan-1-ol; ethanol / 1 h / 50 °C / Inert atmosphere; Large scale

With chloro-trimethyl-silane; sulfuryl dichloride; ammonium acetate; triethylamine; zinc; In tetrahydrofuran; propan-1-ol; ethanol; dichloromethane; tert-butyl methyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;