4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

Base Information

Chemical Name:4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate
CAS No.:1433545-62-0
Molecular Formula:C₁₈H₂₂O₆
Molecular Weight:334.369
Hs Code.:

Synonyms:4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

Suppliers and Price of 4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

Chemical Property:

Boiling Point:485.2±40.0 °C(Predicted)
Density:1.186±0.06 g/cm3(Predicted)

Purity/Quality:: 98% HPLC ^*data from raw suppliers

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Technology Process of 4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

There total 4 articles about 4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4426-03-3
cyclobutyl acetonitrile

: 1433545-62-0
4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc; chloro-trimethyl-silane / tetrahydrofuran / 4 h / 70 °C / Inert atmosphere; Large scale

1.2: 1 h / 20 °C / Large scale

2.1: sulfuryl dichloride / tert-butyl methyl ether / 1.5 h / 20 - 23 °C / Large scale

3.1: triethylamine / N,N-dimethyl-formamide / 14 h / 55 °C / Inert atmosphere; Large scale

With chloro-trimethyl-silane; sulfuryl dichloride; triethylamine; zinc; In tetrahydrofuran; tert-butyl methyl ether; N,N-dimethyl-formamide;

Reference yield:

: 885280-12-6
ethyl 4-cyclobutyl-3-oxobutanoate

: 1433545-62-0
4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl dichloride / tert-butyl methyl ether / 1.5 h / 20 - 23 °C / Large scale

2: triethylamine / N,N-dimethyl-formamide / 14 h / 55 °C / Inert atmosphere; Large scale

With sulfuryl dichloride; triethylamine; In tert-butyl methyl ether; N,N-dimethyl-formamide;

Reference yield:

: 63659-30-3
cyclobutylmethyl methanesulfonate

: 1433545-62-0
4-cyclobutyl-1-ethoxy-1,3-dioxobutan-2-yl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethyl sulfoxide / 4.67 h / 85 °C / Inert atmosphere; Large scale

2.1: zinc; chloro-trimethyl-silane / tetrahydrofuran / 4 h / 70 °C / Inert atmosphere; Large scale

2.2: 1 h / 20 °C / Large scale

3.1: sulfuryl dichloride / tert-butyl methyl ether / 1.5 h / 20 - 23 °C / Large scale

4.1: triethylamine / N,N-dimethyl-formamide / 14 h / 55 °C / Inert atmosphere; Large scale

With chloro-trimethyl-silane; sulfuryl dichloride; triethylamine; zinc; In tetrahydrofuran; tert-butyl methyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;