N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate

Base Information

Chemical Name:N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate
CAS No.:77727-43-6
Molecular Formula:C₂₃H₂₃N₇O₇
Molecular Weight:509.478
Hs Code.:

Synonyms:N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate

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Chemical Property of N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate

Chemical Property:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate

There total 1 articles about N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77716-11-1
4-[(tert-butoxycarbonyl)amino]-1-methyl-1H-pyrrole-2-carboxylic acid

: 77727-43-6
N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / dimethylformamide / 40 °C

2: TFA / CH₂Cl₂

3: EDC / dimethylformamide / 40 °C

4: H₂ / 5percent Pd/C / dimethylformamide / 2 h / 3102.9 Torr / Ambient temperature

5: 88 percent / DCC / dimethylformamide / 1.) 70 min, 0 deg C, 2.) 40 deg C, overnight

With hydrogen; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00330a022

Reference yield:

: 77727-43-6
N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate

: 77152-88-6
(1-amino-3-ammoniopropylidene)ammonium dihydrobromide

: 6576-51-8
distamycin A hydrochloride

Guidance literature:: With hydrogenchloride; sodium hydrogencarbonate; In 1,4-dioxane; water; Yield given; 1.) 15 min, ice-cooled, 2.) room temperature, overnight;
DOI:10.1021/jo00330a022

Reference yield:

: 77727-43-6
N-Succinimidyl 4-<<<4-<<<4-(Formylamino)-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrol-2-yl>carbonyl>amino>-1-methylpyrrole-2-carboxylate

: 85406-94-6
3-Amino-N,N-dimethyl-propionamidine; hydrobromide

: 85407-13-2
C₂₄H₃₁N₉O₄

Guidance literature:: With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; 1.) RT, 1 h, 2.) 40 deg C, 2 h;
DOI:10.1021/jm00361a018