Technology Process of N,N-bis(4-aminophenyl)-2,4-diphenylquinolin-6-amine
There total 4 articles about N,N-bis(4-aminophenyl)-2,4-diphenylquinolin-6-amine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrazine hydrate;
In
ethanol;
at 50 ℃;
for 12.5h;
DOI:10.1002/pola.24250
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid; acetic acid / 4 h / Heating
2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 12 h / Heating
3: cesium fluoride / dimethyl sulfoxide / 18 h / 140 °C
4: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 12.5 h / 50 °C
With
sulfuric acid; palladium 10% on activated carbon; hydrazine hydrate; acetic acid; cesium fluoride;
In
ethanol; dimethyl sulfoxide;
1: Friedlaender synthesis;
DOI:10.1002/pola.24250
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid; acetic acid / 4 h / Heating
2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 12 h / Heating
3: cesium fluoride / dimethyl sulfoxide / 18 h / 140 °C
4: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 12.5 h / 50 °C
With
sulfuric acid; palladium 10% on activated carbon; hydrazine hydrate; acetic acid; cesium fluoride;
In
ethanol; dimethyl sulfoxide;
1: Friedlaender synthesis;
DOI:10.1002/pola.24250
