2',3'-O-Methylene-5'-O,6-N-bisadenosine

Base Information

Chemical Name:2',3'-O-Methylene-5'-O,6-N-bisadenosine
CAS No.:101072-38-2
Molecular Formula:C₄₉H₄₁N₅O₄
Molecular Weight:763.896
Hs Code.:

2',3'-O-Methylene-5'-O,6-N-bis<triphenylmethyl>adenosine

Synonyms:2',3'-O-Methylene-5'-O,6-N-bisadenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',3'-O-Methylene-5'-O,6-N-bisadenosine

Chemical Property:

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Technology Process of 2',3'-O-Methylene-5'-O,6-N-bisadenosine

There total 3 articles about 2',3'-O-Methylene-5'-O,6-N-bisadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 31085-55-9
(2R,3R,4S,5R)-2-(6-(tritylamino)-9H-purin-9-yl)-5-((trityloxy)methyl)tetrahydrofuran-3,4-diol

: 74-95-3
1,1-dibromomethane

: 101072-38-2
2',3'-O-Methylene-5'-O,6-N-bisadenosine

Guidance literature:: With sodium hydroxide; cetyltrimethylammonim bromide; In dichloromethane; for 4.5h; Heating;
DOI:10.1055/s-1985-31332

Reference yield:

: 76-83-5
trityl chloride

: 101072-38-2
2',3'-O-Methylene-5'-O,6-N-bisadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / pyridine / 47 h / 50 - 60 °C

2: 81 percent / aq. NaOH / cetyltrimethylammonium bromide / CH₂Cl₂ / 4.5 h / Heating

With pyridine; sodium hydroxide; cetyltrimethylammonim bromide; In dichloromethane;
DOI:10.1055/s-1985-31332

Reference yield:

: 58-61-7
adenosine

: 101072-38-2
2',3'-O-Methylene-5'-O,6-N-bisadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / pyridine / 47 h / 50 - 60 °C

2: 81 percent / aq. NaOH / cetyltrimethylammonium bromide / CH₂Cl₂ / 4.5 h / Heating

With pyridine; sodium hydroxide; cetyltrimethylammonim bromide; In dichloromethane;
DOI:10.1055/s-1985-31332