sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

Base Information

Chemical Name:sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate
CAS No.:1345614-47-2
Molecular Formula:C₁₄H₁₈NO₄S*Na
Molecular Weight:319.357
Hs Code.:

Synonyms:sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

Suppliers and Price of sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

There total 1 articles about sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1810-74-8
7-methoxy-2,2,4-trimethyl-1,2-dihydroquinoline

: 1345614-47-2
sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 50 °C

2: sulfuric acid; sulfur trioxide / 20 h / 0 - 20 °C

With sulfuric acid; sulfur trioxide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ol202619f

Reference yield: 84.0%

: 1345614-47-2
sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

: 456-27-9
4-nitrobenzenediazonium tetrafluoroborate

: 1345614-48-3
ammonium (7-methoxy-1,2,2-trimethyl-6-(4-nitrophenylazo)-1,2-dihydroquinolin-4-yl)methanesulfonate

Guidance literature:: With sulfuric acid; In methanol; water; at 20 ℃; for 1h;
DOI:10.1021/ol202619f

Reference yield:

: 1345614-47-2
sodium (7-methoxy-1,2,2-trimethyl-1,2-dihydroquinolin-4-yl)methanesulfonate

: 1345614-52-9
(7-methoxy-1,2,2-trimethyl-6-(4-nitrophenylazo)-1,2-dihydroquinolin-4-yl)methanesulfonic acid 2,2,2-trifluoro-1-phenylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus pentachloride; trichlorophosphate / 20 °C

2: triethylamine / dichloromethane / 1 h / 0 °C

3: sulfuric acid / methanol; water / 1 h / 20 °C

With phosphorus pentachloride; sulfuric acid; triethylamine; trichlorophosphate; In methanol; dichloromethane; water;
DOI:10.1021/ol202619f