Cy-vBRIDP

Base Information

• Chemical Name: Cy-vBRIDP
• CAS No.: 384842-24-4
• Molecular Formula: C27H35 P
• Molecular Weight: 390.549
• DSSTox Substance ID: DTXSID40475778
• Nikkaji Number: J2.532.036K
• Mol file: 384842-24-4.mol

Synonyms:Cy-vBRIDP;384842-24-4;Cy-vBRIDP(regR);dicyclohexyl(1,1-diphenylprop-1-en-2-yl)phosphane;Dicyclohexyl(1,1-diphenylprop-1-en-2-yl)phosphine;Dicyclohexyl(1-methyl-2,2-diphenylethenyl)phosphine;MFCD10565627;Dicyclohexyl(2,2-diphenyl-1-methylvinyl)phosphine;Dicyclohexyl(1,1-diphenyl-1-propen-2-yl)phosphine;SCHEMBL377393;DTXSID40475778;YMSBPYCREGBACF-UHFFFAOYSA-N;AKOS025295265;C2981;CS-0035265;1,1-Diphenyl-2-(dicyclohexylphosphino)propene;T70863

Chemical Property of Cy-vBRIDP

Chemical Property:

• Melting Point: 124-130 °C
• PSA: 13.59000
• LogP: 8.61320
• Storage Temp.: 2-8°C
• Sensitive.: air sensitive, store cold
• Water Solubility.: Insoluble in water
• XLogP3: 7.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 5
• Exact Mass: 390.247638114
• Heavy Atom Count: 28
• Complexity: 444

Purity/Quality:

98% ^*data from raw suppliers

Cy-vBRIDP[R] >90.0%(HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CC(=C(C1=CC=CC=C1)C2=CC=CC=C2)P(C3CCCCC3)C4CCCCC4
• Uses: Catalyst for cycloaddition reactions

Technology Process of Cy-vBRIDP

There total 1 articles about Cy-vBRIDP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-bromo-1,1-diphenylpropene (781-32-8) + chlorodicyclohexylphosphane (16523-54-9) → dicyclohexyl(1,1-diphenyl-1-propen-2-yl)phosphine (384842-24-4)

Guidance literature:

2-bromo-1,1-diphenylpropene; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 0.5h;

chlorodicyclohexylphosphane; In tetrahydrofuran; hexane; at -70 - 20 ℃; for 16.75h;

Reference yield: 98.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + dicyclohexyl(1,1-diphenyl-1-propen-2-yl)phosphine (384842-24-4) → PdCl2(cyclohexyl-(1,1-diphenylprop-1-en-2-yl)phophine)2

Guidance literature:

In toluene; at 30 ℃; for 3h; Inert atmosphere;

DOI:10.1002/adsc.201300332

Reference yield:

potassium phosphate + dicyclohexyl(1,1-diphenyl-1-propen-2-yl)phosphine (384842-24-4) + p-tolyl triflate (29540-83-8) + ammonium chloride + p-toluidine (106-49-0,12221-03-3) → di-p-tolylamine (620-93-9)

Guidance literature:

In 1,4-dioxane;

upstream raw materials:

2-bromo-1,1-diphenylpropene

chlorodicyclohexylphosphane

Downstream raw materials:

4-morpholinobenzonitrile

N-(4-methylphenyl)-4-methoxyaniline

di-p-tolylamine

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