N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate

Base Information

Chemical Name:N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate
CAS No.:1071927-61-1
Molecular Formula:C₂₀H₁₇Cl₂F₃N₂O₃
Molecular Weight:461.268
Hs Code.:

Synonyms:N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate

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Chemical Property of N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate

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Technology Process of N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate

There total 5 articles about N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1071927-10-0
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylaniline

: 541-41-3
chloroformic acid ethyl ester

: 1071927-61-1
N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 31680-07-6
4-methyl-3-nitrobenzaldehyde

: 1071927-61-1
N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1 h / 20 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 50 °C

3: triethylamine / N,N-dimethyl-formamide / 6 h / 20 °C

4: acetic acid / iron / ethanol; water / 1.25 h / 75 °C

5: triethylamine / tetrahydrofuran / 2 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; sodium acetate; acetic acid; triethylamine; iron; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: C₈H₇ClN₂O₃

: 1071927-61-1
N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-3-isoxazolyl)-2-methylphenyl)-O-ethyl-carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 6 h / 20 °C

2: acetic acid / iron / ethanol; water / 1.25 h / 75 °C

3: triethylamine / tetrahydrofuran / 2 h / 20 °C

With acetic acid; triethylamine; iron; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;