(1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

Base Information

Chemical Name:(1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine
CAS No.:236115-91-6
Molecular Formula:C₄₃H₄₇N₁₅O₆
Molecular Weight:869.943
Hs Code.:

(1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

Synonyms:(1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

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Chemical Property of (1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

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Technology Process of (1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

There total 3 articles about (1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 236115-81-4
5-O-allyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzyl neamine

: 236115-91-6
(1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

Guidance literature:: Multi-step reaction with 2 steps

1: O₃; S(CH₃)2

2: NaCNBH₃ / acetic acid

With dimethylsulfide; sodium cyanoborohydride; ozone; In acetic acid; 1: Oxidation / 2: Condensation;
DOI:10.1002/(SICI)1521-3773(20000317)39:6<1080::AID-ANIE1080>3.0.CO;2-B

Reference yield:

: 5805-57-2
2-Aminomethylbenzimidazole

: 236115-82-5
[(1R,2R,3S,5R,6S)-3,5-Diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-acetaldehyde

: 236115-91-6
(1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

Guidance literature:: With sodium cyanoborohydride; In methanol; acetic acid; for 2h; Yield given; Ambient temperature;
DOI:10.1021/ja9910356

Reference yield:

: 236115-80-3
1,3,2',6'-tetraazido-6,3',4'-tri-O-benzyl neamine

: 236115-91-6
(1H-Benzoimidazol-2-ylmethyl)-{2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-ethyl}-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaH, tetrabutylammonium iodide / dimethylformamide / 2 h / Ambient temperature

2: 1.) O₃, 2.) Me₂S / 1.) CH₂Cl₂, MeOH, -78 deg C, 20 s, 2.) CH₂Cl₂, MeOH, RT, 1 h

3: NaCNBH₃ / methanol; acetic acid / 2 h / Ambient temperature

With dimethylsulfide; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; ozone; In methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ja9910356