1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate

Base Information

Chemical Name:1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate
CAS No.:1357159-20-6
Molecular Formula:C₉H₁₁O₃S*C₂₆H₃₀N₃O₂
Molecular Weight:615.794
Hs Code.:

Synonyms:1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate

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Chemical Property of 1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate

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Technology Process of 1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate

There total 5 articles about 1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1357159-18-2
tert-butyl 1-(4-(3-phenylpyridin-2-yl)phenyl)cyclobutylcarbamate

: 36016-40-7
mesitylenesulfonylhydroxylamine

: 1357159-20-6
1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 7h; Inert atmosphere;
DOI:10.1021/jm201394e

Reference yield:

: 52200-48-3
3-bromo-2-chloropyridine

: 1357159-20-6
1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / cyclopentyl methyl ether; water / 3 h / 65 °C / Inert atmosphere

2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; potassium carbonate / acetonitrile / 6 h / 80 °C / Inert atmosphere

3: dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium carbonate; potassium carbonate; In dichloromethane; cyclopentyl methyl ether; water; acetonitrile;
DOI:10.1021/jm201394e

Reference yield:

: 31557-57-0
2-chloro-3-phenyl-pyridine

: 1357159-20-6
1-amino-2-(4-(1-(tert-butoxycarbonylamino)cyclobutyl)phenyl)-3-phenylpyridinium 2,4,6-trimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; potassium carbonate / acetonitrile / 6 h / 80 °C / Inert atmosphere

2: dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1021/jm201394e