(E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide

Base Information

Chemical Name:(E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide
CAS No.:1373438-16-4
Molecular Formula:C₂₃H₁₈BrN₃O₂
Molecular Weight:448.319
Hs Code.:

Synonyms:(E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide

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Technology Process of (E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide

There total 3 articles about (E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1373439-01-0
1-(5-phenyl-1H-indol-2-yl)ethanone

: 39635-10-4
2-hydroxy-5-bromobenzohydrazide

: 1373438-16-4
(E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide

Guidance literature:: In propan-1-ol; Reflux;
DOI:10.1016/j.bmc.2012.10.002

Reference yield: 92.0%

: 1373438-16-4
(E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide

Guidance literature:

Reference yield:

: 89671-83-0
1-(5-bromo-1H-indol-2-yl)ethan-1-one

: 98-80-6
phenylboronic acid

: 1373438-16-4
(E)-5-bromo-2-hydroxy-N'-(1-(5-phenyl-1H-indol-2-yl)ethylidene)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / Inert atmosphere; Reflux

2: propan-1-ol / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In propan-1-ol; 1,2-dimethoxyethane; water;
DOI:10.1016/j.bmc.2012.10.002