[(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane

Base Information

Chemical Name:[(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane
CAS No.:182949-14-0
Molecular Formula:C₂₃H₄₀O₂Si
Molecular Weight:376.655
Hs Code.:

Synonyms:[(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane

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Chemical Property of [(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane

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Technology Process of [(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane

There total 3 articles about [(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-39-0
benzyl bromide

: 182949-13-9
(3R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-3,7-dimethyl-oct-6-en-1-ol

: 182949-14-0
[(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 2h; Ambient temperature;
DOI:10.1039/p19960002291

Reference yield:

: 144781-81-7
methyl (3S,4R)-4-(tert-butyldimethylsiloxy)-3,7-dimethyl-6-octenoate

: 182949-14-0
[(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 0 °C

2: 100 percent / NaH / dimethylformamide / 2 h / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/p19960002291

Reference yield:

: 144781-72-6
(1R,2R,3R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(1-chloro-1-methyl-ethyl)-2-methyl-cyclopentanecarboxylic acid methyl ester

: 182949-14-0
[(R)-1-((R)-3-Benzyloxy-1-methyl-propyl)-4-methyl-pent-3-enyloxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: SmI₂ / tetrahydrofuran; hexamethylphosphoric acid triamide / Ambient temperature

2: 93 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 0 °C

3: 100 percent / NaH / dimethylformamide / 2 h / Ambient temperature

With lithium aluminium tetrahydride; samarium diiodide; sodium hydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide;
DOI:10.1039/p19960002291