diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese

Base Information

Chemical Name:diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese
CAS No.:75602-16-3
Molecular Formula:C₃₅H₂₈MnO₄PSn
Molecular Weight:717.227
Hs Code.:

Synonyms:diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese

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Chemical Property of diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese

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Technology Process of diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese

There total 2 articles about diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 15279-67-1,10170-70-4
dimanganese octacarbonyl di-(triphenyl phosphine)

: 4167-84-4
diphenyl methyl tin chloride

: 75602-16-3
diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese

Guidance literature:: With NaHg(x); In tetrahydrofuran; byproducts: NaCl; (N2), to cooled NaHg(x) added THF and (Mn(CO)4PPh3)2, mixture stirred for 24 h, added to soln. of Sn-compound in THF under N2 (through a filtercovered with glasswool), mixture stirred at room temp. for 12 h; NaCl centrifuged, soln. evapd., chromd. (SiO2, C6H6/petroleum ether (2/1) at 40°C), crystd. with n-hexane, elem. anal.;

Reference yield: 25.0%

: 19457-74-0
sodium tetracarbonyl(triphenylphosphine)manganate(-I)

: 75602-17-4
(CH₃)(C₆H₅)2Sn(Co(CO)3P(C₆H₅)3)

: 75602-16-3
diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese

Guidance literature:: In tetrahydrofuran; soln. of Ph3P(CO)4MnNa in THF added to soln. of Ph2MeSnCo(CO)3PPh3 in THF under N2, reaction time 12 h; solvent evapd., chromd., NMR, IR;

Reference yield: 100.0%

: sodium dicarbonyl(cyclopentadienyl)ferrate

: 75602-16-3
diphenylmethylstannyltetracarbonyl(triphenylphosphine)manganese

: (CH₃)(C₆H₅)2SnFe(CO)2(C₅H₅)

Guidance literature:: In tetrahydrofuran; soln. of (C5H5)(CO)2FeNa in THF added to soln. of Ph2MeSnMn(CO)4PPh3 inTHF under N2, reaction time 12 h; solvent evapd., chromd., NMR, IR;