1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene

Base Information

• Chemical Name: 1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene
• CAS No.: 438497-33-7
• Molecular Formula: C₁₉H₂₄O₂SSe
• Molecular Weight: 395.424

Synonyms:1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene

Chemical Property of 1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene

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Technology Process of 1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene

There total 3 articles about 1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R,3S,4R)-4-methoxy-3-(2-methoxy-6-[(1S)-1-(methylsulfanyl)ethyl]phenylselanyl)-4-phenylbutan-2-ol (819852-48-7) + styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → 1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene (438497-33-7)

Guidance literature:

With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃;

DOI:10.1021/ol048001+

Reference yield:

(2R,3S,4R)-4-(4-chlorophenyl)-4-methoxy-3-(2-methoxy-6-[(1S)-1-(methylsulfanyl)ethyl]phenylselanyl)butan-2-ol (819852-54-5) + styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → 1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene (438497-33-7)

Guidance literature:

With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃;

DOI:10.1021/ol048001+

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + methanol (67-56-1) + C10H14O5S2Se (438497-45-1) → 1-methoxy-2-{[(2R)-2-methoxy-2-phenylethyl]seleno}-3-[(1S)-1-(methylthio)ethyl]benzene (438497-33-7)

Guidance literature:

In dichloromethane; at -30 ℃; for 24h;

DOI:10.1002/1521-3765(20020301)8:5<1118::AID-CHEM1118>3.0.CO;2-2

upstream raw materials:

styrene

methanol

C₁₀H₁₄O₅S₂Se

(2R,3S,4R)-4-methoxy-3-(2-methoxy-6-[(1S)-1-(methylsulfanyl)ethyl]phenylselanyl)-4-phenylbutan-2-ol

Downstream raw materials:

(S)-(-)-1-methoxy-1-phenylethane

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