(Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene

Base Information

Chemical Name:(Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene
CAS No.:1109183-47-2
Molecular Formula:C₁₇H₁₅ClF₂O₃S
Molecular Weight:372.82
Hs Code.:

Synonyms:(Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene

Suppliers and Price of (Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene

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Technology Process of (Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene

There total 1 articles about (Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1109183-31-4
(E)-(1,1-difluoro-3-iodo-4-methoxybut-2-enylsulfonyl)benzene

: 1679-18-1
4-Chlorophenylboronic acid

: 1109183-47-2
(Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; at 65 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.tet.2008.11.011

Reference yield: 52.0%

: 1109183-47-2
(Z)-1-chloro-4-(4,4-difluoro-1-methoxy-4-(phenylsulfonyl)but-2-en-2-yl)benzene

: 1109183-64-3
(Z)-1-chloro-4-(4,4-difluoro-1-methoxybut-2-en-2-yl)benzene

Guidance literature:: With sodium acetate; magnesium; acetic acid; In water; N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1016/j.tet.2008.11.011