N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide

Base Information

Chemical Name:N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide
CAS No.:1367872-50-1
Molecular Formula:C₂₁H₃₀N₄O₂
Molecular Weight:370.495
Hs Code.:

Synonyms:N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide

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Chemical Property of N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide

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Technology Process of N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide

There total 8 articles about N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1367874-81-4
2-[4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl]ethanamine

: 98-89-5
Cyclohexanecarboxylic acid

: 1367872-50-1
N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1246347-08-9
4-(cyclohexyloxy)-3-methyl-1H-pyrazolo[4,3-c]pyridine

: 1367872-50-1
N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dmap / acetonitrile / 1 h / 20 °C

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux

3.1: ethanol; water / 4 h / 20 °C

4.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Cooling with ice

4.2: 1 h / -10 °C

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; dibenzoyl peroxide; dmap; In tetrachloromethane; diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 120422-93-7
4-chloro-3-methylpyrazolo<4,2-c>pyridine

: 1367872-50-1
N-(2-(4-(cyclohexyloxy)-1H-pyrazolo[4,3-c]pyridin-3-yl)ethyl)cyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / 1,4-dioxane; mineral oil / 1 h / 20 °C / Sealed microwave vial

1.2: 2 h / 20 - 190 °C / Microwave irradiation

2.1: triethylamine / dmap / acetonitrile / 1 h / 20 °C

3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux

4.1: ethanol; water / 4 h / 20 °C

5.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Cooling with ice

5.2: 1 h / -10 °C

6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; dibenzoyl peroxide; dmap; In 1,4-dioxane; tetrachloromethane; diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;