2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

Base Information

Chemical Name:2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide
CAS No.:246862-24-8
Molecular Formula:C₂₃H₃₆O₃S
Molecular Weight:392.603
Hs Code.:

Synonyms:2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

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Chemical Property of 2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

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Technology Process of 2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

There total 6 articles about 2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 246862-23-7
(3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate

: 246862-24-8
2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(99)01242-3

Reference yield:

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 246862-24-8
2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

Guidance literature:: Multi-step reaction with 5 steps

1: LiAlH₄ / diethyl ether / 4 h / Heating

2: Et₃N / methanol

3: 85 percent / LiOH / tetrahydrofuran / 7 h / 20 °C

4: 95 percent / N,N'-carbonyldiimidazole / CH₂Cl₂ / 36 h / 20 °C

5: 85 percent / BF₃*OEt₂ / CH₂Cl₂ / 2 h / 0 °C

With lithium hydroxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)00078-3

Reference yield:

: 22693-41-0
2,4,6-Triisopropylthiophenol

: 246862-24-8
2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / methanol

2: 85 percent / LiOH / tetrahydrofuran / 7 h / 20 °C

3: 95 percent / N,N'-carbonyldiimidazole / CH₂Cl₂ / 36 h / 20 °C

4: 85 percent / BF₃*OEt₂ / CH₂Cl₂ / 2 h / 0 °C

With lithium hydroxide; boron trifluoride diethyl etherate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)00078-3