(3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate

Base Information

• Chemical Name: (3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate
• CAS No.: 246862-23-7
• Molecular Formula: C₂₃H₃₆O₃S
• Molecular Weight: 392.603

Synonyms:(3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate

Chemical Property of (3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate

Chemical Property:

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Technology Process of (3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate

There total 6 articles about (3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3-hydroxymethyl-3-methyloxethane (3143-02-0) + 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionic acid (246862-22-6) → (3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate (246862-23-7)

Guidance literature:

With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 36h;

DOI:10.1016/S0040-4020(01)00078-3

Reference yield:

2,4,6-triisopropylphenylsulfonyl chloride (6553-96-4) → (3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate (246862-23-7)

Guidance literature:

Multi-step reaction with 4 steps

1: LiAlH₄ / diethyl ether / 4 h / Heating

2: Et₃N / methanol

3: 85 percent / LiOH / tetrahydrofuran / 7 h / 20 °C

4: 95 percent / N,N'-carbonyldiimidazole / CH₂Cl₂ / 36 h / 20 °C

With lithium hydroxide; lithium aluminium tetrahydride; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;

DOI:10.1016/S0040-4020(01)00078-3

Reference yield:

2,4,6-Triisopropylthiophenol (22693-41-0) → (3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate (246862-23-7)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N / methanol

2: 85 percent / LiOH / tetrahydrofuran / 7 h / 20 °C

3: 95 percent / N,N'-carbonyldiimidazole / CH₂Cl₂ / 36 h / 20 °C

With lithium hydroxide; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1016/S0040-4020(01)00078-3

upstream raw materials:

3-hydroxymethyl-3-methyloxethane

3-[(2,4,6-triisopropylphenyl)sulfenyl]propionic acid

2,4,6-triisopropylphenylsulfonyl chloride

2,4,6-Triisopropylthiophenol

Downstream raw materials:

(S)-2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfoxide

(R)-2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfoxide

2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfoxide

2-(4-methyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)ethyl 2,4,6-triisopropylphenyl sulfide

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