prenyl tributylstannane

Base Information

Chemical Name:prenyl tributylstannane
CAS No.:104108-29-4
Molecular Formula:C₁₇H₃₆Sn
Molecular Weight:359.183
Hs Code.:

Synonyms:prenyl tributylstannane

Suppliers and Price of prenyl tributylstannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of prenyl tributylstannane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of prenyl tributylstannane

There total 3 articles about prenyl tributylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 53911-92-5,104108-29-4
2-methylbut-3-en-2-yl(tributyl)stannane

: 93415-08-8
Benzyl 3-iodopropanoate

: 104108-29-4
prenyl tributylstannane

: 108957-11-5
benzyl 6-methylhept-5-enoate

Guidance literature:: With catalyst: azobisisobutyronitrile; In toluene; refluxed for 48 h;
DOI:10.1039/c39860001339

Reference yield:

: 1461-22-9
tributyltin chloride

: 870-63-3
prenyl bromide

: 53911-92-5,104108-29-4
2-methylbut-3-en-2-yl(tributyl)stannane

: 115991-75-8
2-methyl-2-butenyltributyltin

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; water; appropriate alkyltin chloride is added to THF/H2O mixt. with excess of zinc powder, appropriate allyl bromide is added dropwise under stirring within 5 min, mixt. is stirred for 30 min; extn. (petroleum ether), separated org. layer is washed (aq. NaCl), drying (MgSO4), solvent is removed, distn., mixt. of isomers 3-methyl-1-buten-3-yltributyltin and 2-methyl-2-butenyltributyltin ratio 40:60; total yield 62%;
DOI:10.1021/om00015a025

Reference yield:

: 104108-29-4
prenyl tributylstannane

: 53911-92-5,104108-29-4
2-methylbut-3-en-2-yl(tributyl)stannane

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; In benzene; Irradiation (UV/VIS); N2; Sn-compd. soln. irradiation with 300 W high-pressure Hg lamp throughsatd. aq. CuSO4 soln. (280 nm) for 3 h, solvent evapn. (reduced pressur e);
DOI:10.1039/a707609f