Technology Process of C13H17N3O3S
There total 6 articles about C13H17N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; acetic acid;
at 70 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dmap / 0 - 20 °C
2: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide / N,N-dimethyl-formamide / 20 - 70 °C
3: water; acetic acid / 70 °C
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; water; acetic acid;
dmap;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: magnesium sulfate / (1S)-10-camphorsulfonic acid / acetone / 5 h / 20 °C
2: magnesium sulfate; Dess-Martin periodane / dichloromethane / 8 h / 20 °C
3: tetrahydrofuran / 2.5 h / -30 °C
4: pyridine / dmap / 0 - 20 °C
5: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide / N,N-dimethyl-formamide / 20 - 70 °C
6: water; acetic acid / 70 °C
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; water; magnesium sulfate; Dess-Martin periodane; acetic acid;
dmap; (1S)-10-camphorsulfonic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;