diphenyltrifluoromethylphosphine oxide

Base Information

Chemical Name:diphenyltrifluoromethylphosphine oxide
CAS No.:16284-64-3
Molecular Formula:C₁₃H₁₀F₃OP
Molecular Weight:270.191
Hs Code.:

Synonyms:diphenyltrifluoromethylphosphine oxide

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Chemical Property of diphenyltrifluoromethylphosphine oxide

Chemical Property:

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Technology Process of diphenyltrifluoromethylphosphine oxide

There total 4 articles about diphenyltrifluoromethylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1605-56-7
(trifluoromethyl)-diphenylphosphine

: 16284-64-3
diphenyltrifluoromethylphosphine oxide

Guidance literature:: With dihydrogen peroxide; In water; acetone;

Reference yield:

: 119-61-9
benzophenone

: 129922-46-9
triphenyl(trifluoromethyl)phosphonium trifluoromethanesulfonate

: 16284-64-3
diphenyltrifluoromethylphosphine oxide

: 1605-56-7
(trifluoromethyl)-diphenylphosphine

Guidance literature:: With Dimethylphenylsilane; In dichloromethane; at 100 ℃; for 4h; Inert atmosphere; Sealed tube;
DOI:10.1039/c7cc09128a

Reference yield:

: 13360-92-4
phenyl diphenylphosphinite

: 16284-64-3
diphenyltrifluoromethylphosphine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: cesium fluoride / diethyl ether / 18 h / 20 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 5,5-dimethyl-1,3-cyclohexadiene / 40 h / 145 °C / Inert atmosphere; Sealed tube

3: Dimethylphenylsilane / dichloromethane / 4 h / 100 °C / Inert atmosphere; Sealed tube

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; Dimethylphenylsilane; cesium fluoride; In 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; dichloromethane;
DOI:10.1039/c7cc09128a