tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate

Base Information

Chemical Name:tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate
CAS No.:1356349-81-9
Molecular Formula:C₂₀H₃₁FN₂O₂
Molecular Weight:350.477
Hs Code.:

Synonyms:tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate

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Chemical Property of tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate

Chemical Property:

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Technology Process of tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate

There total 6 articles about tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82420-35-7
2-(bromomethyl)-4-fluoro-1-nitrobenzene

: 1356349-81-9
tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / acetonitrile

2: triethylamine / dichloromethane / 0 - 25 °C

3: hydrazine hydrate / Raney Nickel / methanol / 0 - 25 °C

With hydrazine hydrate; caesium carbonate; triethylamine; Raney Nickel; In methanol; dichloromethane; acetonitrile;

Reference yield:

: 1356349-79-5
tert-butyl [(2S)-1-cyclopentylpropan-2-yl](5-fluoro-2-nitrobenzyl)carbamate

: 1356349-81-9
tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate

Guidance literature:: With hydrazine hydrate; Raney Nickel; In methanol; at 0 - 25 ℃;

Reference yield:

: 446-33-3
5-Fluoro-2-nitrotoluene

: 1356349-81-9
tert-butyl (2-amino-5-fluorobenzyl)[(2S)-1-cyclopentylpropan-2-yl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 50 - 80 °C

2: caesium carbonate / acetonitrile

3: triethylamine / dichloromethane / 0 - 25 °C

4: hydrazine hydrate / Raney Nickel / methanol / 0 - 25 °C

With N-Bromosuccinimide; hydrazine hydrate; caesium carbonate; triethylamine; dibenzoyl peroxide; Raney Nickel; In methanol; tetrachloromethane; dichloromethane; acetonitrile;