tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate

Base Information

Chemical Name:tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate
CAS No.:1432059-82-9
Molecular Formula:C₂₃H₂₁Cl₂N₃O₃
Molecular Weight:458.344
Hs Code.:

Synonyms:tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate

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Technology Process of tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate

There total 11 articles about tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 7677-24-9
trimethylsilyl cyanide

: 1432059-19-2
C₂₂H₂₀Cl₂N₂O₃

: 1432059-82-9
tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate

Guidance literature:: With 1-(3,5-bis(trifluoromethyl)phenyl)-3-((R)-quinolin-4-yl((1S,2R,4S,5R)-5-vinylquinu clidin-2-yl)methyl)thiourea; 1,1,1,3',3',3'-hexafluoro-propanol; In dichloromethane; at -70 ℃; enantioselective reaction;
DOI:10.1039/c2cc36665g

Reference yield:

: C₂₇H₃₀Cl₂N₄O₃

: 1432059-82-9
tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 30 ℃; for 0.00833333h;
DOI:10.1021/acs.orglett.0c01857

Reference yield:

: 7677-24-9
trimethylsilyl cyanide

: 1432059-19-2
C₂₂H₂₀Cl₂N₂O₃

: 1432059-42-1
(R,E)-tert-butyl {3-cyano-1-[3-(3,4-dichlorophenyl)allyl]-2-oxoindolin-3-yl}carbamate

: 1432059-82-9
tert-butyl (E)-(3-cyano-1-(3-(3,4-dichlorophenyl)allyl)-2-oxoindolin-3-yl)carbamate

Guidance literature:: With C₂₈H₂₆F₆N₄S; 1,1,1,3',3',3'-hexafluoro-propanol; Triphenylphosphine oxide; In 1,2-dichloro-ethane; at -30 ℃; for 24h; enantioselective reaction;
DOI:10.1039/c2cc36665g