N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester

Base Information

• Chemical Name: N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester
• CAS No.: 100677-59-6
• Molecular Formula: C₁₀H₁₁ClN₂O₂
• Molecular Weight: 226.663

Synonyms:N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester

Chemical Property of N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester

Chemical Property:

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Technology Process of N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester

There total 1 articles about N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrazinecarboxylic acid methyl ester (6294-89-9) + 1-chloroacetophenone (532-27-4,108321-66-0,164322-25-2) → N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester (100677-59-6)

Guidance literature:

for 3h; Yield given; Ambient temperature;

DOI:10.1055/s-1985-31424

Reference yield: 86.0%

4-bromonitrosobenzene (3623-23-2) + N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester (100677-59-6) → (1Z,2Z)-N-(4-bromophenyl)-2-(2-(methoxycarbonyl)hydrazono)-2-phenylethan-1-imine oxide

Guidance literature:

With sodium carbonate; In dichloromethane; at 20 ℃; for 26h; stereoselective reaction;

DOI:10.1055/a-1509-0949

Reference yield: 70.0%

N'-[2-Chloro-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester (100677-59-6) + Nitrosobenzene (586-96-9) → (1Z,2Z)-2-(2-(methoxycarbonyl)hydrazono)-N,2-diphenylethan-1-imine oxide

Guidance literature:

With sodium carbonate; In dichloromethane; at 20 ℃; for 24h; stereoselective reaction;

DOI:10.1055/a-1509-0949

upstream raw materials:

hydrazinecarboxylic acid methyl ester

1-chloroacetophenone

Downstream raw materials:

N'-[2-(Diphenyl-phosphinoyl)-1-phenyl-eth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester

[2-(Methoxycarbonyl-hydrazono)-2-phenyl-ethyl]-phosphonic acid dimethyl ester

[2-(Methoxycarbonyl-hydrazono)-2-phenyl-ethyl]-phosphonic acid diethyl ester

phenacyldiphenylphosphine oxide

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