2-hydrohexafluoropropyl fluorosulfate

Base Information

• Chemical Name: 2-hydrohexafluoropropyl fluorosulfate
• CAS No.: 684-35-5
• Molecular Formula: C₃HF₇O₃S
• Molecular Weight: 250.094
• Mol file: 684-35-5.mol

Synonyms:2-hydrohexafluoropropyl fluorosulfate

Chemical Property of 2-hydrohexafluoropropyl fluorosulfate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-hydrohexafluoropropyl fluorosulfate

There total 3 articles about 2-hydrohexafluoropropyl fluorosulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

perfluoropropylene (116-15-4,13429-24-8,25120-07-4,6792-31-0) → perfluoroisopropyl iodide (677-69-0) + 2-hydrohexafluoropropyl fluorosulfate (684-35-5) + 2-iodo-hexafluoropropyl fluorosulfate (77570-01-5)

Guidance literature:

With iodine; antimony pentafluoride; fluorosulphonic acid; at 20 ℃; for 72h;

DOI:10.1007/BF00963248

Reference yield:

perfluoropropylene (116-15-4,13429-24-8,25120-07-4,6792-31-0) → 1,1,1,2,3,3,3-Heptafluoropropane (431-89-0) + 2-hydrohexafluoropropyl fluorosulfate (684-35-5)

Guidance literature:

With antimony pentafluoride; fluorosulphonic acid; at 20 ℃; for 12h; Yields of byproduct given;

DOI:10.1007/BF00963248

Reference yield:

perfluoropropylene (116-15-4,13429-24-8,25120-07-4,6792-31-0) → 1,2-dibromohexafluoropropane (661-95-0) + 2-bromo-1,1,1,2,3,3,3-heptafluoropropane (422-77-5) + 2-bromohexafluoropropyl fluorosulfate (41255-95-2) + 2-hydrohexafluoropropyl fluorosulfate (684-35-5)

Guidance literature:

With bromine; antimony pentafluoride; fluorosulphonic acid; for 48h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1007/BF00963248

upstream raw materials:

perfluoropropylene

Downstream raw materials:

2-hydroperfluoropropionamide

Refernces